A Two-Stage Cascading Amplification Strategy Based on Zn(2+)-Doped WO(X) Nanozymes for Ultrasensitive Lateral Flow Immunoassays of Clostridium Difficile Toxin B

基于Zn(2+)掺杂WO(X)纳米酶的两阶段级联放大策略用于艰难梭菌毒素B的超灵敏侧向流动免疫测定

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Abstract

Clostridium difficile is one of the primary causative agents of nosocomial antibiotic-associated diseases. Early detection and prevention are effective strategies to curb disease transmission, which often requires highly sensitive point-of-care testing (POCT) methods. Although lateral flow immunoassay (LFIA) technology-known for its convenience, speed, and cost-effectiveness-has gained prominence in POCT, its application in early screening remains limited due to relatively low sensitivity. Herein, a two-stage cascading enhancement strategy based on reductase-like and peroxidase-like activities of nanozyme to construct a colorimetrically enhanced LFIA platform is proposed. Specifically, Zn(2+)-doped WO(X) (Zn/WO(X)) loaded with Au nanoparticles (Zn/WO(X)@Au) first generates an initial colorimetric signal through immunochromatography. Subsequently, in situ light-induced deposition of Pt creates Zn/WO(X)@Au@Pt, which exhibits enhanced peroxidase-like activity based on optimal band structure between the components for colorimetric signal amplification. As a result, a 500-fold enhancement in the visual limit of detection (LOD) is achieved. Moreover, the fitted LOD based on grayscale analysis for Clostridium difficile toxin B (Tcd B) reaches 0.01 ng mL(-1). This strategy not only maintains the operational simplicity of LFIA but also considerably strengthens the colorimetric signal, offering a novel approach for highly sensitive colorimetric-enhanced LFIA detection.

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