Synthesis and Characterization of Polynorbornenes with Nitronaphthyl Side-Chains

含硝基萘侧链的聚降冰片烯的合成与表征

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Abstract

Three new norbornene monomers carrying naphthyl-based sidechains with varying levels of electron deficiency are synthesized, characterized by (1)H NMR, 2D-NMR, UV-vis, and fluorescence spectroscopies, as well as mass spectrometry. The kinetics of their ring-opening polymerization using a third-generation Grubbs catalyst are established, and the resulting polymers are characterized by size-exclusion chromatography, along with UV-vis and fluorescence spectroscopies. These naphthalene-based polynorbornenes are shown to exhibit fluorescence, accompanied by a quenching behavior when exposed to an electron-rich aromatic compound.

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