Cobalt(II)-Mediated Fenton-like Reactions: Effects of Second-Sphere H(2)O(2) and Thiolate Coordination

钴(II)介导的类芬顿反应:第二配位层H₂O₂和硫醇盐配位的影响

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Abstract

While the Co(II) aqua complex is not a good catalyst for H(2)O(2) decomposition due to its high redox potential, the Fenton-like activity of Co(II) can be promoted by chelation with suitable ligands. Previous experiments have shown that different reactive oxygen species (ROS) are generated in the presence of different ligands, but the underlying mechanism is unclear. In this study, density functional theory calculations are used to investigate the decomposition of H(2)O(2) mediated by Co(II) complexes containing nitrilotriacetate (NTA), ethylenediaminetetraacetate (EDTA), and glutathione (GSH). For the NTA- and EDTA-Co(II) complexes, the formation of free (•)OH via the conventional Fenton-like pathway is thermodynamically unfavorable. However, H(2)O(2) accumulated in the second coordination sphere via hydrogen bonding with carboxylate groups can readily undergo hydrogen atom transfer with (•)OH produced from the coordinated H(2)O(2), generating (•)OOH as the major ROS. This reaction step provides a thermodynamic driving force for the H(2)O(2) decomposition, which we call the second-sphere H(2)O(2)-assisted Fenton-like reaction. On the other hand, the conventional Fenton-like reaction of the GSH-Co(II) complex is kinetically and thermodynamically favorable, generating (•)OH as the major ROS. Detailed analysis reveals that the thiolate group of GSH plays a dominant role in promoting the conventional Fenton-like reaction.

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