Automated synthesis of (R)-[(18) F]MH.MZ on the iPhase Flexlab reaction platform

在 iPhase Flexlab 反应平台上自动合成 (R)-[(18)F]MH.MZ

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Abstract

(R)-[(18) F]MH.MZ ([(18) F]MH.MZ) is a promising positron emission tomography (PET) radiotracer for in vivo study of the 5-HT(2A) receptor. To facilitate clinical trials, a fully automated radiosynthesis procedure for [(18) F]MH.MZ was developed using commercially available materials on the iPhase Flexlab module. The overall synthesis time was 100 min with a radiochemical yield of 7 ± 0.9% (n = 3). The radiochemical purity was greater than 99% for [(18) F]MH.MZ with a molar activity of 361 ± 57 GBq/μmol (n = 3). The protocol described herein reliably provides [(18) F]MH.MZ that meets all relevant release criteria for a GMP radiopharmaceutical.

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