Abstract
Precise design of graphitic carbon nitride (gC(3)N(4)) nanostructures is of grand importance in different catalytic applications. This article emphasizes additional data on the fabrication of metal-free gC(3)N(4) nanofibres (gC(3)N(4)NFs) and its associated structural and composition analysis compared with Au/Pd co-doped gC(3)N(4) nanofibres (Au/Pd/gC(3)N(4)NFs). The data is including the typical fabrication process of metal-free gC(3)N(4) nanofibers and its SEM, TEM, and element mapping analysis beside Raman, and FTIR spectra relative to Au/Pd/gC(3)N(4)NFs. We also investigated the catalytic CO oxidation durability testes on Au/Pd/gC(3)N(4)NFs compared to Pd/gC(3)N(4)NFs and Au/gC(3)N(4)NFs. The presented data are associated with the research article entitled "Rational synthesis of one-dimensional carbon nitride-based nanofibers atomically doped with Au/Pd for efficient carbon monoxide oxidation." [1].