Abstract
The data presented in this article are related to the research article entitled "Hierarchical yolk-shell CNT-(NiCo)O_C microspheres prepared by one-pot spray pyrolysis as anodes in lithium-ion batteries" (Oh et al., 2019). The data presented in this manuscript showed the effect of the reaction temperature during spray pyrolysis on the obtained microspheres morphology. Each morphology and phase of the microspheres obtained after spray pyrolysis were investigated.