A one-dimensional coordination polymer, catena-poly[[[[N-ethyl-N-(pyridin-4-ylmeth-yl)di-thio-carbamato-κ(2)S,S']zinc(II)]-μ(2)-N-ethyl-N-(pyridin-4-ylmeth-yl)di-thio-carbamato-κ(3)S,S':N] 4-methyl-pyridine hemisolvate]

一维配位聚合物,catena-poly[[[[N-乙基-N-(吡啶-4-基甲基)二硫代氨基甲酸酯-κ(2)S,S']锌(II)]-μ(2)-N-乙基-N-(吡啶-4-基甲基)二硫代氨基甲酸酯-κ(3)S,S':N]4-甲基吡啶半溶剂化物]

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Abstract

The title compound, {[Zn(C(9)H(11)N(2)S(2))(2)]·0.5C(6)H(7)N} (n) , comprises two independent, but chemically similar, Zn[S(2)CN(Et)CH(2)py](2) residues and a 4-methyl-pyridine solvent mol-ecule in the asymmetric unit. The Zn-containing units are connected into a one-dimensional coordination polymer (zigzag topology) propagating in the [010] direction, with one di-thio-carbamate ligand bridging in a μ(2)-κ(3) mode, employing one pyridyl N and both di-thio-carbamate S atoms, while the other is κ(2)-chelating. In each case, the resultant ZnNS(4) coordination geometry approximates a square pyramid, with the pyridyl N atom in the apical position. In the crystal, the chains are linked into a three-dimensional architecture by methyl- and pyridyl-C-H⋯S, methyl-ene-C-H⋯N(pyrid-yl) and pyridyl-C-H⋯π(ZnS(2)C) inter-actions. The connection between the chain and the 4-methyl-pyridine solvent mol-ecule is of the type pyridyl-C-H⋯N(4-methyl-pyridine).

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