Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography

利用同步辐射X射线多尺度断层扫描技术观察维氏压痕法在玻璃陶瓷中引起的亚表面裂纹的形貌

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Abstract

The characterization of subsurface cracks induced by indentation is a challenge for understanding contact damage, impact, wear, erosion, and abrasion of brittle materials, because the crack pattern observable on the surface is only a part of the total crack system. Here we applied synchrotron X-ray multiscale tomography to observe the morphology of subsurface cracks produced by Vickers indentation in a novel CaO-Al(2)O(3)-SiO(2) glass-ceramic with plate-like crystals forming a house-of-cards microstructure. It revealed a diverse type of crack systems around the semispherical microcrack zone beneath the indent, including a new mode II inclined lateral crack driven by the maximum shear stress. Tomography images provided knowledge on how the heterogeneous microstructure affected the toughening processes such as crack deflection, crack bridging, and microcracking.

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