Shrinkage, Degree of Conversion, Water Sorption and Solubility, and Mechanical Properties of Novel One-Shade Universal Composite

新型单色通用复合材料的收缩率、转化率、吸水性和溶解度以及力学性能

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Abstract

This study aims to evaluate the shrinkage, degree of conversion, water sorption and solubility, and mechanical properties of a newly developed one-shade universal composite and compare it with five other commercially available universal composites with one or multiple shades. Our proprietary resin and filler technologies developed the experimental one-shade universal composite (Experimental). Volumetric shrinkage was determined using the AcuVol video imaging method (n = 5). Degree of conversion was measured using FTIR (n = 5). Water sorption and solubility (15 × 1 mm, n = 5) and flexural strength and modulus (2 × 2 × 25 mm, n = 5) were measured according to ISO-4049. Diametral tensile strength (6 × 3 mm, n = 8) was tested according to ANSI/ADA-Specification #27. The data were analyzed using one-way ANOVA and post hoc Tukey tests (p ≤ 0.05). Like Clearfil Majesty ES-2, Experimental showed lower or significantly lower volumetric shrinkage than other composites. Experimental exhibited a considerably higher degree of conversion and high flexural modulus compared to the others. However, there are no significant differences in flexural strength among these universal composites except for Omnichroma. Experimental also displayed significantly higher diametral tensile strength than the others, except similar to Filtek Supreme Ultra. Experimental has the lowest values of water sorption and solubility among the composites tested. The experimental universal composite demonstrated improved or comparable physical and mechanical properties compared to commercially available one-shade universal composites or multi-shade conventional universal composites, which is of significance for the clinical performance of dental restorations.

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