Effect of Metal Oxides on the Pyrolytic Behavior and Combustion Performance of 5-Aminotetrazole/Sodium Periodate Gas Generators in Atmospheric Environment

金属氧化物对大气环境下5-氨基四唑/高碘酸钠气体发生器热解行为和燃烧性能的影响

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Abstract

5-aminotetrazole (5AT)-based gas generators, particularly the 5AT/NaIO(4) system, have garnered interest for their high gas production and energy potential. This study investigates the impact of various metal oxides (MnO(2), Al(2)O(3), TiO(2), CuO, Fe(2)O(3), MgO, ZnO, and MoO(3)) on the thermal decomposition and combustion performance of 5AT/NaIO(4). The REAL calculation program was used to infer reaction products, which indicated that the gas products are almost all harmless, with negligibly low percentages of NO and CO. Thermogravimetric analysis revealed that metal oxides, especially MoO(3), significantly advance the decomposition process above 400 °C, reducing the activation energy by 130 kJ/mol and lowering critical ignition and thermal explosion temperatures. Combustion performance tests and closed bomb tests confirmed MoO(3)'s positive effect, accelerating reaction rates and enhancing decomposition efficiency. The system's high Gibbs free energy indicates non-spontaneous reactions. These findings provide valuable insights for designing environmentally friendly gas generators, highlighting MoO(3)'s potential as an effective catalyst.

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