Crystal structure and Hirshfeld surface analysis of a supra-molecular aggregate of 4-formyl-N,N-di-methyl-anilinium bromide with tetra-bromomethane

4-甲酰基-N,N-二甲基苯胺溴化物与四溴甲烷超分子聚集体的晶体结构和Hirshfeld表面分析

阅读:1

Abstract

The title compound, C(9)H(12)NO(+)·Br(-)·CBr(4), consists of one 4-formyl-N,N-di-methyl-benzenaminium bromide and a tetra-bromo-methane mol-ecule. In the crystal, the bromide ions link 4-formyl-N,N-di-methyl-benzenaminium moieties through inter-molecular C-H⋯Br and N-H⋯Br hydrogen bonds, while inter-molecular C-H⋯O hydrogen bonds link 4-formyl-N,N-di-methyl-benzenaminium cations, enclosing R (2) (2)(18) ring motifs, into a di-periodic network structure. The tetra-bromo-methane mol-ecules fill the spaces between the layers. Neither π-π nor C-H⋯π(ring) inter-actions are observed. A Hirshfeld surface analysis of the crystal structure indicates that the most abundant contacts contributing to the crystal packing are from H⋯Br/Br⋯H (56.0%), Br⋯Br (12.1%), H⋯O/O⋯H (9.7%) and H⋯H (9.5%) inter-actions.

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。