Effect of Freckle Defects on Hot Deformation Behavior and Dynamic Recrystallization Structure Inheritance of an Iron-Nickel-Based Superalloy

斑点缺陷对铁镍基高温合金热变形行为和动态再结晶组织继承的影响

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Abstract

To study the influence of freckle defects on the hot deformation behavior and the inheritance of dynamic recrystallization (DRX) structure in GH4706 alloy, the microstructures of specimens with and without freckles and the evolution laws of hot-processing parameters were compared. Hot compression experiments were conducted on a thermal simulation testing machine at 950-1150 °C, strain rates of 0.001-1 s(-1), and 55% deformation. Freckle-containing specimens were tested under DRX critical conditions. The flow stresses of both specimens increase with strain rate or with decreasing temperature. The power dissipation coefficient (η) and instability value (ξ) follow complex laws. Electron back-scattering diffraction (EBSD) was used to analyze DRX microstructures and nucleation mechanisms. The DRX degree of freckle-containing specimens is lower, with a larger average grain size. The DRX mechanism initiates preferentially in freckle-containing specimens, and its volume fraction changes in a complex manner. Grain coarsening occurs in freckle-containing specimens at high temperatures and low strain rates. Freckle defects lead to significant differences in the DRX mechanism of GH4706 alloy. Freckle-containing specimens exhibit both discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX), whereas freckle-free specimens primarily display DDRX and second-phase particle-stimulated nucleation (PSN). The presence of MC carbides and Laves phases within freckle defects provides nucleation sites, further supporting a typical second-phase particle-stimulated nucleation mechanism.

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