Microstructural Analysis of Hot-Compressed Mg-Nd-Zr-Ca Alloy with Low Rare-Earth Content

低稀土含量热压Mg-Nd-Zr-Ca合金的微观结构分析

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Abstract

Microstructural analysis of hot-compressed magnesium alloys is crucial for understanding the plastic formability of magnesium alloys during thermo-mechanical processing. Thermal compression tests and finite element simulations were conducted on a low rare-earth (RE) Mg-1.8Nd-0.4Zr-0.3Ca alloy. Multiple microstructural characterization techniques were employed to analyze slip systems, twinning mechanisms, dynamic recrystallization (DRX), and precipitate phases in the hot-compressed alloy. The results demonstrated that the equivalent strain distribution within compressed specimens exhibits heterogeneity, with a larger equivalent strain in the core. After thermal compression, the original microscopic structure formed a necklace-like structure. The primary DRX mechanisms comprise continuous dynamic recrystallization (CDRX), twin-induced dynamic recrystallization (TDRX), and particle-stimulated nucleation (PSN). Pyramidal slip and recrystallization constitute primary contributors to peak texture weakening and tilting. Mg(4)(1)Nd(5) and α-Zr phases enhanced dislocation density by impeding dislocation motion and promoting cross-slip activation. Hot compression provided the necessary thermal activation energy and stress conditions for solute atom diffusion and clustering, triggering dynamic precipitation of Mg(4)(1)Nd(5) phases.

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