Synthesis and crystal structure of poly[(2,6-di-methyl-py-ra-zine-κN (4))(μ(3)-thiocyanato-κ(3) N:S:S)copper(I)]

聚[(2,6-二甲基-吡啶-嗪-κN(4))(μ(3)-硫氰酸根-κ(3)N:S:S)铜(I)]的合成和晶体结构

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Abstract

Crystals of the title compound, [Cu(NCS)(C(6)H(8)N(2))] (n) (C(6)H(8)N(2) = 2,6-di-methyl-pyrazine), were prepared by the reaction of CuNCS and 2,6-di-methyl-pyrazine in aceto-nitrile. The asymmetric unit consists of one Cu(I) cation, one thio-cyanate anion and one 2,6-di-methyl-pyrazine ligand with all atoms lying on general positions. The copper cations are tetra-hedrally coordinated by two S- and one N-bonded thio-cyanate anions and one 2,6-di-methyl-pyrazine ligand, which s coordinated to the metal center with the N atom that is not adjacent to the methyl groups. The copper cations are linked by the μ-1,3,3 (N,S,S) bridging thio-cyanate anions into layers that lie parallel to the ac plane. The layers are stacked perpendicular to the b-axis direction and are separated by the 2,6-di-methyl-pyrazine ligands. The title crystal structure is compared with those of related CuNCS compounds with isomeric di-methyl-pyrazine ligands.

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