Synthesis and crystal structure of bis-[μ(2)-7-({bis-[(pyridin-2-yl)meth-yl]amino-κ(3) N,N',N''}meth-yl)-5-chloro-quinolin-8-olato-κ(2) N,O]dizinc(II) bis-(perchlorate) aceto-nitrile monosolvate

双-[μ(2)-7-({双-[(吡啶-2-基)甲基]氨基-κ(3)N,N',N''}甲基)-5-氯喹啉-8-醇盐-κ(2)N,O]二锌(II)双(高氯酸盐)乙腈单溶剂化物的合成及晶体结构

阅读:1

Abstract

The title compound, [Zn(2)(C(22)H(18)ClN(4)O)(2)](ClO(4))(2)·CH(3)CN, consists of one centrosymmetric cationic dinuclear zinc(II) complex with two penta-dentate ligands containing quinolin-8-olato and bis-(pyridin-2-ylmeth-yl)amine groups, two perchlorate counter-ions and one aceto-nitrile solvate mol-ecule. The Zn(II) atom adopts a distorted octa-hedral geometry and coordinates the O atom and the N atom of the quinolin-8-olato group and three N atoms of the bis-(pyridin-2-ylmeth-yl)amine group in a ligand, and the O atom in an adjacent ligand generated by an inversion operation. The phenolato oxygen atoms in the two ligands of the cationic dinuclear complex are bridging coordinated with the two Zn(II) atoms. In the crystal, the cationic dinuclear complex mol-ecules and perchlorate ions are linked by C-H⋯Cl and C-H⋯O hydrogen bonds, forming a three-dimensional network.

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。