Microstructural Evolution and Internal Hydrogen Content of Ultra-High-Strength Automotive Steels During Two Typical Industrial Production Flows

两种典型工业生产流程中超高强度汽车钢的微观结构演变和内部氢含量

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Abstract

Hot stamping is a promising method to manufacture ultra-high-strength automotive steel components with high dimension accuracy. In this work, two actual industrial production flows (with and without Al-Si hot dipping) were investigated to reveal their microstructural evolution and hydrogen content at different production steps. Meanwhile, the variations in composition and phase structures of the Al-Si coating layer were studied in terms of energy-dispersive spectrometry and electron backscattering diffraction techniques. The results showed that the microstructure at the steel substrate changed from the pancake-shaped pearlite and ferrite, degenerated pearlite and annealed ferrite, lath martensite, and then tempered martensite with the progress of the production steps, which was not affected by the Al-Si hot dipping. The final coating layer exhibited a multi-sublayer structure with the alternative distribution of FeAl and Fe(2)Al(5), which contained many microcracks on the brittle phase Fe(2)Al(5). The Al-Si-coated specimens always had higher hydrogen content than the bare steel specimens because of the hydrogen generation at the hot stamping stage and hydrogen absorption during the hot-dip aluminizing stage.

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