Design, Synthesis, and Biological Evaluation of Tetrazol-2-yl-acetamides as Novel Antitubercular Agents

四唑-2-基乙酰胺类化合物作为新型抗结核药物的设计、合成及生物学评价

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Abstract

A focused small-molecule library was screened against extracellular Mycobacterium tuberculosis (Mtb) across four distinct carbon sources that mimic different metabolic states of the pathogen. This screen identified a novel tetrazol-2-yl-acetamide compound, sALT629 (P1), with potent intramacrophage activity (EC(50) = 1.5 μM). sALT629 showed broad-spectrum activities across all carbon sources, equipotent efficacy against drug-resistant Mtb, and activity against both slow-replicating and nonreplicating Mtb. Structure-activity relationship (SAR) studies optimized the potency and drug-like properties, leading to analogue P39 with improved intramacrophage activity (EC(50) = 0.68 μM) and pharmacokinetics (PK) properties. In mice, P39 achieved a plasma exposure of 58,754 ng/mL and maintained plasma concentrations above EC(50) for 16 h after a 20 mg/kg oral dose. Additionally, sALT629 showed good exposure and tolerability after repeated dosing for 4 days at 200 mg/kg once daily (QD) or 100 mg/kg twice daily (BID), indicating low toxicity liability and the potential for further development as an anti-tuberculosis (TB) drug candidate.

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