Compound Analysis and Mechanistic Exploration of Shen-Yan-Fang-Shuai Formula in Diabetic Kidney Disease: An UHPLC-MS/MS and Bioinformatics Study

肾炎防帅方治疗糖尿病肾病的成分分析及机制探讨:一项基于超高效液相色谱-串联质谱(UHPLC-MS/MS)和生物信息学的研究

阅读:1

Abstract

BACKGROUND: Diabetic kidney disease (DKD) is significantly impacting both quality of life and survival rates. The Shen-Yan-Fang-Shuai (SYFS) formula is a traditional Chinese medicine (TCM) compound widely used in the clinical treatment of DKD with proven efficacy, though its potential mechanism of action remains unclear. This study attempts to elucidate the therapeutic efficacy, mechanisms of action, and active compounds of the SYFS formula in the treatment of DKD. MATERIALS AND METHODS: The components of SYFS formula were identified by UHPLC-MS/MS. Differentially expressed genes (DEGs) and key module genes were selected based on the GEO database to obtain intersection targets. Protein-protein interaction (PPI) network and component-target network were constructed. Machine learning (ML) was employed to screen for hub genes, which were validated through nomogram, immune infiltration analysis, molecular docking and molecular dynamics (MD) simulation. Subsequently, our findings were validated through a combination of transcriptomic sequencing of renal tissue from animal models and real-time quantitative PCR (qPCR) analyses performed on both the animal tissues and HK-2 cells. RESULTS: 154 chemical components and 994 targets were identified in the SYFS formula. Intersection with DEGs and WGCNA module genes identified 39 potential targets. Five hub genes (MMP3, MMP12, PTGES, SST, and DUSP1) were selected through ML and used to construct a nomogram. Multiple immune cell infiltration levels were significantly elevated in DKD, with hub genes showing correlations with specific immune cell types. Molecular docking and MD simulation validated the binding capacity between components of the SYFS formula and key targets. In addition, it has been further verified in animal experiments and cell experiments. CONCLUSIONS: The core components of the SYFS formula, including naringenin chalcone, palmatine, oleanonic acid, β-elemonic acid, and Naringenin, likely exert their effects through the MMP3, MMP12, PTGES, SST, and DUSP1 targets. This research offers empirical support for the application of the SYFS formula in DKD, establishing a crucial groundwork for subsequent clinical investigations.

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。