Surface Roughness and Color Stability of Conventional Glass Ionomer Cement Reinforced With a Nanofiller Synthesized by the Coprecipitation Method

采用共沉淀法合成纳米填料增强的常规玻璃离子水门汀的表面粗糙度和颜色稳定性研究

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Abstract

AIM: Modification of conventional glass ionomer cement (GIC) using nanofillers is a promising approach to enhance its clinical performance. This study aimed to evaluate the surface roughness and color stability of conventional GIC after modification with a synthesized 70:30 hydroxyapatite/chitosan (HA/CTS) nanocomposite. MATERIALS AND METHODS: A 70:30 hydroxyapatite/chitosan nanocomposite was synthesized and incorporated into GIC powder at 1, 3, and 5 wt.%. Four groups were prepared: Group I (control), Group II (1 wt.% HA/CTS), Group III (3 wt.% HA/CTS), and Group IV (5 wt.% HA/CTS). A total of 80 specimens were fabricated (n = 10 per group for each test). Surface roughness (Ra) was measured using a profilometer, while color stability (ΔE) was assessed using a spectrophotometer. Data were analyzed using one‐way ANOVA followed by Tukey’s post hoc test (α = 0.05). RESULTS: GIC modified with the 3 wt.% HA/CTS nanocomposite exhibited the lowest surface roughness and demonstrated clinically acceptable color change (ΔE ≤ 3.3) (p < 0.05). Higher nanocomposite loading (5 wt.%) resulted in significantly increased surface roughness and clinically perceptible color alteration. CONCLUSIONS: Incorporation of the 3 wt.% 70:30 HA/CTS nanocomposite into conventional GIC produced a smoother surface and acceptable esthetic outcome, suggesting a promising formulation for improved clinical performance.

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