Orthogonal Design Optimisation of the Sintering Process for MnZn Ferrites with Step-Sintering Verification

采用正交设计优化方法对锰锌铁氧体烧结工艺进行优化及逐步烧结验证

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Abstract

MnZn ferrites for power electronics require a well-controlled sintering window to balance high initial permeability (µ(i)) with low power loss (P(cv)). Here, an L9 (3(3)) orthogonal design was employed to quantify the main effects of sintering temperature, holding time, and oxygen partial pressure on µ(i) and P(cv) within the investigated processing window, enabling rapid mapping of feasible sintering windows. The orthogonal analysis identifies the relative significance of each factor and reveals a clear performance trade-off between µ(i) and P(cv). For maximising µ(i), the optimal sintering condition was 1250 °C, 4 h holding time, and 3.5% oxygen partial pressure, yielding a µ(i) of 3453 and a P(cv) of 466 mW/cm(3) at 100 kHz/200 mT. For minimising P(cv), the optimal condition was 1250 °C, 3.5 h holding time, and 5% oxygen partial pressure, resulting in a µ(i) of 2678, with P(cv) of 400 mW/cm(3) at 100 kHz/200 mT and 182 mW/cm(3) at 500 kHz/50 mT. Targeted verification together with XRD, SEM grain-size statistics, and magnetic-loss separation were used to strengthen the process-structure-property interpretation. Overall, the orthogonal-screening-plus-verification strategy provides a practical framework for predicting application-relevant performance trends of MnZn ferrites within a defined processing window.

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