Fe(3)O(4)@SiO(2)-LY-C-D-Pd as a new, effective, and magnetically recoverable catalyst for the synthesis of 1H-tetrazoles and asymmetric biphenyls

Fe(3)O(4)@SiO(2)-LY-CD-Pd 作为一种新型、高效且磁性可回收的催化剂,用于合成 1H-四唑和不对称联苯

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Abstract

This research project explored the synthesis and characterization of a newly developed C-D-Pd complex immobilized on Fe(3)O(4)@SiO(2)-LY, designed as a reusable magnetic catalyst. The heterogeneous nanocatalyst was thoroughly characterized using EDS, FTIR, XRD, XPS, TGA, SEM, VSM, and ICP techniques. The Fe(3)O(4)@SiO(2)-LY-C-D-Pd catalyst demonstrates exceptional performance in catalyzing C-C coupling reactions and (1)H-tetrazole derivatives, achieving high product yields. This catalyst offers several advantages, including eco-friendly reaction conditions, minimal catalyst usage, a simple experimental setup, the elimination of harmful organic solvents, reduced reaction times, and the ability to accommodate diverse substrates. Additionally, the nanocatalyst is easily separable from the reaction mixture and can be reused multiple times without losing stability or catalytic efficiency.

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