Interlayer Modification of Crystalline Layered Silicates with Oligodimethylsiloxane

低聚二甲基硅氧烷对结晶层状硅酸盐进行层间改性

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Abstract

Crystalline layered silicates are valuable precursors for the synthesis of functional siloxane-based nanomaterials. In this study, vinyl-terminated oligodimethylsiloxane was grafted onto the interlayer surfaces of a crystalline layered silicate, octosilicate. The oligosiloxane modification facilitated the delamination of the layers in hydrophobic organic solvents. Hydrosilylation reactions between the oligosiloxane-modified nanosheets and SiH-terminated polydimethylsiloxane resulted in a clear, stretchable elastomer, demonstrating that the nanosheets acted as cross-linkers. Furthermore, the introduction of silanolate groups into the elastomer imparted self-healing properties. These findings expand the potential of crystalline layered silicates as nanobuilding blocks for new materials.

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