Crystal structure and Hirshfeld surface analysis of a pyridiniminium bromide salt: 1-[2-([1,1'-biphen-yl]-4-yl)-2-oxoeth-yl]-3-methyl-1,4-di-hydro-pyridin-4-iminium bromide

吡啶亚胺溴化物盐的晶体结构和Hirshfeld表面分析:1-[2-([1,1'-联苯基]-4-基)-2-氧代乙基]-3-甲基-1,4-二氢吡啶-4-亚胺溴化物

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Abstract

In the cation of the title salt, C(20)H(19)N(2)O(+)·Br(-), the phenyl rings are inclined to one another by 38.38 (8)°, whereas the central phenyl ring and the pyridiniminium ring are almost perpendicular with a dihedral angle of 87.37 (9)°. The N(+)=C cationic double bond was verified by the shortened bond length of 1.337 (2) Å. In the crystal, the Br(-) anion is linked to the cation by an N-H⋯Br hydrogen bond. C-H⋯O hydrogen bonds link adjacent pyridiniminium cations into inversion dimers with an R(2)(2)(18) graph-set motif. These dimers are stacked in a phen-yl-phenyl T-shaped geometry through C-H⋯π inter-actions. A Hirshfeld surface analysis was conducted to verify the contributions of the different inter-molecular inter-actions.

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