Crystal structure of di-μ-hydroxido-bis-{aqua-[ethyl (1,10-phenanthrolin-3-yl)phospho-nato-κ(2) N,N']copper(II)} hepta-hydrate

二-μ-羟基-双-{水-[乙基(1,10-菲咯啉-3-基)磷酸-nato-κ(2)N,N']铜(II)}七水合物的晶体结构

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Abstract

In the title compound, [Cu(2)(OH)(2){C(12)H(7)N(2)(PO(3)C(2)H(5))}(2)(H(2)O)(2)]·7H(2)O, two Cu(2+) cations are bridged by two hydroxide groups, forming a centrosymmetric binuclear complex. Each Cu(2+)cation is further coordinated by the N atoms of a bidentate ethyl (1,10-phenanthrolin-3-yl)phospho-nate anion and a water mol-ecule in a square-pyramidal geometry. In the crystal, a network of O-H⋯O hydrogen bonds involving the P(O)(O(-))(OEt) groups, bridging hydroxyl groups, coordinated and uncoordinated water mol-ecules generates a three-dimensional supra-molecular structure. The ethyl group exhibits disorder and was modelled over three sites with occupancies of 0.455, 0.384 and 0.161.

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