Effect of Indenter Load on Vickers Microhardness and Indentation Depth of One Resin Composite

压头载荷对一种树脂复合材料维氏显微硬度和压痕深度的影响

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Abstract

The load and size of the indentation may affect the hardness value. This study investigated the effect of the indentation size on the microhardness of one resin-based composite (RBC). Metal molds 4 mm deep and 12 mm in diameter were filled with Tetric EvoCeram Bulk Fill (Ivoclar) and light-cured for 10 s using a broad-spectrum LED curing light. The Vickers microhardness and the degree of conversion (DC) at the top and bottom surfaces were measured 24 h later before and after polishing the RBC. The microhardness measurements were made using 50, 100, 300 and 1000-gf loads with the same 8 s dwell time. The DC was measured in the same region using mid FT-IR spectroscopy. Repeated measures analysis of variance tests were used to determine if the surface (top vs. bottom) or the indenter loads had a significant effect on the VH, or if polishing affected the VH and the DC (alpha = 0.05). It was found that the indenter load did not affect the Vickers hardness of the unpolished top surface (p = 0.759), the polished top surface (p = 0.374), or the polished bottom surface (p = 0.083) of the Tetric EvoCeram Bulk Fill. Increasing the indenter load did increase the VH of the unpolished surface at the bottom (p < 0.0001). Polishing increased the DC by 13.5% at the top and by 46.7% at the bottom surface.

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