Solubility and Thermodynamics Data of Cabozantinib Malate in Various Aqueous Solutions of Dimethyl Sulfoxide at Different Temperatures

卡博替尼苹果酸盐在不同温度下于二甲基亚砜水溶液中的溶解度和热力学数据

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Abstract

Cabozantinib malate (CBZM), a new anticancer medication, has been studied for its solubility and thermodynamic properties in a variety of {dimethyl sulfoxide (DMSO) + water (H(2)O)} mixtures at 298.2-318.2 K and 101.1 kPa. Using the shake flask technique, the solubility of CBZM was assessed and the results were correlated to the van't Hoff, Apelblat, Buchowski-Ksiazczak λh, Yalkowsky-Roseman, Jouyban-Acree, and Jouyban-Acree-van't Hoff models. There was a significant correlation between the experimental CBZM solubility data and all computational models, as evidenced by the error values for all computational models being less than 5.0%. Temperature and DMSO mass percentage improved the CBZM mole fraction solubility in the cosolvent solutions of {DMSO + H(2)O}. At 318.2 K, pure DMSO had the highest mole fraction solubility of CBZM (4.38 × 10(-2)), whereas pure H(2)O had the lowest mole fraction solubility (2.24 × 10(-7) at 298.2 K). The positive values of computed thermodynamic parameters indicated that the dissolution of CBZM was endothermic and entropy-driven in all of the {DMSO + H(2)O} solutions investigated. It was found that the CBZM solvation in {DMSO + H(2)O} solutions is governed by enthalpy. When compared to CBZM-H(2)O, CBZM-DMSO showed the highest molecular interactions. The findings of this investigation demonstrated that DMSO has a great deal of potential for CBZM solubilization in H(2)O.

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