Extraction with SPME and synthesis of 2-methyl-6-vinylpyrazine by a 'one pot' reaction using microwaves

采用 SPME 萃取并通过微波“一锅式”反应合成 2-甲基-6-乙烯基吡嗪

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作者:Norma Robledo, Jaime Escalante, René Arzuffi

Abstract

A synthesis of 2-methyl-6-vinylpyrazine was carried out by way of a 'one pot' reaction. In order to establish the efficiency of this synthesis the extraction of the volatiles released by male papaya fruit flies was performed by SPME (solid phase micro-extraction). The compound was separated and identified using GC/MSD (gas chromatography/mass spectrometry detector).

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