The complete mol-ecule of the title compound, C24H28N4O4, is generated by crystallographic inversion symmetry. The ethyl side chain is disordered over two sets of sites in a 0.57â (4):0.43â (4) ratio. The dihedral angles between the methyl-idene group and the phenyl ring and ester side chain (major conformation) are 7.61â (8) and 86.95â (8)°, respectively. In the crystal, mol-ecules are linked via C-Hâ¯O hydrogen bonds, forming corrugated sheets lying parallel to (010).
Diethyl (E)-2,3-bis-[(E)-(2-methyl-2-phenyl-hydrazin-1-yl-idene)meth-yl]but-2-enedioate.
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作者:Liu Peng, Yuan Libin, Song Xiuqing, Yan Hong
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2014 | 起止号: | 2014 May 31; 70(Pt 6):o723 |
| doi: | 10.1107/S1600536814011970 | ||
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