The title compound, C(24)H(23)N(3)O(3)S(2), crystallizes with two independent mol-ecules in the asymmetric unit. They differ essentially in the orientation of the tolyl rings, between which there is Ï-Ï stacking (centroid-centroid distance = 3.01â à ). The absolute configuration was confirmed by the determination of the Flack parameter [x = 0.008â (9)]. In the crystal, mol-ecules are connected by two classical N-Hâ¯N hydrogen bonds and two weak but very short C-Hâ¯O(sulfon-yl) inter-actions, forming layers lying parallel to the bc plane.
(S)-N-[1-(5-Benzyl-sulfan-yl-1,3,4-oxa-diazol-2-yl)-2-phenyl-eth-yl]-4-methyl-benzene-sulfonamide.
(S)-N-[1-(5-苄基硫基-1,3,4-噁二唑-2-基)-2-苯基乙基]-4-甲基苯磺酰胺
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作者:Syed Tayyaba, Hameed Shahid, Jones Peter G
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Nov;67(Pt 11):o2875-6 |
| doi: | 10.1107/S1600536811040669 | ||
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