The asymmetric unit of the title compound, C(13)H(10)F(2)N(2)O, contains one and a half N,N'-bis-(4-fluoro-phen-yl)urea mol-ecules. One of the mol-ecules has crystallographic twofold rotation symmetry. The benzene rings are twisted from each other by dihedral angles of 29.69â (6)° for the mol-ecule in a general position and 89.83â (6)° for the symmetry-generated mol-ecule. In the crystal structure, a pair of inter-molecular N-Hâ¯O hydrogen bonds link symmetry-related mol-ecules into chains along the b axis, forming R(2) (1)(6) ring motifs.
N,N'-Bis(4-fluoro-phen-yl)urea.
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作者:Loh Wan-Sin, Fun Hoong-Kun, Sarveswari S, Vijayakumar V, Ragavan R Venkat
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2010 | 起止号: | 2010 May 12; 66(Pt 6):o1319 |
| doi: | 10.1107/S1600536810016399 | ||
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