Fabrication of Nitrogen-Doped Reduced Graphene Oxide Modified Screen Printed Carbon Electrode (N-rGO/SPCE) as Hydrogen Peroxide Sensor

制备氮掺杂还原氧化石墨烯修饰丝网印刷碳电极(N-rGO/SPCE)作为过氧化氢传感器

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Abstract

In recent years, the electrochemical sensing approach has attracted electrochemists because of its excellent detection process, simplicity, high sensitivity, cost-effectiveness, and high selectivity. In this study, we prepared nitrogen doped reduced graphene oxide (N-rGO) and characterized it using various advanced techniques such as XRD, SEM, EDX, Raman, and XPS. Furthermore, we modified the active surface of a screen printed carbon electrode (SPCE) via the drop-casting of N-rGO. This modified electrode (N-rGO/SPCE) exhibited an excellent detection limit (LOD) of 0.83 µM with a decent sensitivity of 4.34 µAµM(-1)cm(-2) for the detection of hydrogen peroxide (H(2)O(2)). In addition, N-rGO/SPCE also showed excellent selectivity, repeatability, and stability for the sensing of H(2)O(2). Real sample investigations were also carried out that showed decent recovery.

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