Effect of gold nanoparticles and γ-cyclodextrin polymer on physicochemical, antimicrobial, and antibiofilm properties of a novel schiff base derived from dialdehyde cellulose and camphor thiazole-imine

金纳米粒子和γ-环糊精聚合物对由二醛纤维素和樟脑噻唑亚胺衍生的新型席夫碱的理化性质、抗菌性能和抗生物膜性能的影响

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Abstract

The present study developed a novel antimicrobial composite based on 2,3-dialdehyde cellulose (DAC), with biocompatible properties and long-term stability. Initially, DAC was synthesized through the periodate oxidation of microcrystalline cellulose, achieving a 61% degree of oxidation. Subsequently, the DAC was successfully modified through the formation of a Schiff base with CTI in the basic medium. The antimicrobial efficacy of the synthesized DAC-CTI was strengthened by the synthesis of Au NPs via a green chemical approach using lemon extract and their subsequent grafting into the DAC-CTI matrix, followed by encapsulation of the produced DAC-CTI/Au nanocomposite into the γ-cyclodextrin ring. The TEM results of DAC-CTI/Au nanocomposite indicated an average Au particle size of 37.4 nm within the nanocomposite. The evaluated samples reveal a positive efficacy against a variety of bacteria, including P. aeruginosa, C. albicans, and S. aureus. Particularly, DAC-CTI/Au NPs/γ-CD exhibited the highest effect on S. aureus (19.0 mm zone of inhibition (ZOI) and 2.5 µg/mL MIC), E. coli (20.0 mm ZOI and 1.25 µg/mL MIC), and C. albicans (18.2 mm ZOI and 2.5 µg/mL MIC). The outcomes achieved open the door to the practical implementation of intriguing compounds in biological fields.

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