Understanding Ash Sintering Variation Behaviors of Low-Rank Coals with Municipal Sludge Addition Based on Mineral Interactions

基于矿物相互作用理解添加市政污泥对低阶煤灰烧结变化行为的影响

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Abstract

Co-gasification with coal provides an economically viable way to use sludge. To investigate the effect of municipal sludge (MS) on the sintering behaviors of low-rank coals (LRCs) and their modification mechanisms, the initial sintering temperature (T (s)) of three LRCs and their mixtures with MS addition were tested by a T (s) analyzer, an X-ray diffractometer, and FactSage calculation. The results show that the T (s) values of Xiaolongtan coal (XLT), Xiangyuan coal (XY), and Daliuta coal (DLT) all increase with MS addition. The 9-12% MS mass ratio is suitable during LRC fluidized-bed gasification to mitigate ash-related issues. The T (s) is closely related to the liquid-phase content or the transmissions of microparticles (e.g., atoms and ions) or blank spots during heating, while the ash fusion temperatures (AFTs) are mainly determined by acid/base ratios. The T (s) values of high-Fe XLT and XY mixed ashes increased gradually with increasing MS proportion because the sintering mechanisms transferred from liquid phase to solid phase, while for relatively high-Mg DLT ashes, the T (s) values increased with increasing MS proportions, which might result from the formations of high-melting-point minerals (e.g., Ca(3)(PO(4))(2) and Mg(2)SiO(4)). The results deepen the understanding of ash sintering behaviors and provide references to alleviate ash-related issues during gasification.

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