Quantification of Sensitization in Aluminum-Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation

通过频率相关的超声衰减量化铝镁合金的敏化作用

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Abstract

Aluminum-Magnesium (Al-Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al(2)Mg(3)) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al-Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study introduces a time-frequency analysis (TFA) technique to determine the frequency-dependent ultrasonic attenuation parameter and correlate the frequency-attenuation slope to the Degree of Sensitization (DoS) developed in heat-treated Al-Mg alloy samples. Broadband pitch-catch signal was generated using a laser ultrasonic testing (LUT) system, from which the narrowband pitch-catch signal at different frequencies can be digitally generated. The attenuation parameters of sensitized Al-Mg samples were determined from these narrowband pitch-catch signals using the primary pulse-first echo (PP-FE) method. By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. The experimental results validate that the frequency-attenuation slope has a higher sensitivity and lower scattering as compared to other conventional ultrasonic attenuation measurement techniques.

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