A comparison of dentin bond strength and degree of polymerization of bulk-fill and methacrylate-based flowable composites

比较大块填充型和甲基丙烯酸酯基流动型复合材料的牙本质粘接强度和聚合度

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Abstract

OBJECTIVE: This study aimed to evaluate the dentin bond strength and degree of polymerization of bulk-fill and methacrylate-based flowable composites. MATERIALS AND METHODS: Dentin bond strength of composites was evaluated using the microtensile bond strength (μTBS) test. Five different composites were applied on flat dentin surfaces with self-etch and etch-and-rinse adhesives. Twenty microspecimens with a 1 mm(2) cross-sectional area were prepared for each group (n = 20). The μTBS test was then applied. To measure the degree of polymerization of composites, eight cylindrical blocks were prepared (n = 8) from each composite. The surface microhardness of each composite was measured on the bottom and top surfaces, and a hardness ratio (HR) was calculated. Data were analyzed using one-way ANOVA and the Tukey's honestly significant difference test (α = 0.05). RESULTS: According to the μTBS test results, the SDR Etch-and-Rinse group exhibited the highest dentin bonding strength and the Aelita self-etch group exhibited the lowest (P < 0.05). HR measurement showed that all composite groups had a sufficient degree of polymerization at a 2-mm thickness, while only the SDR and Xtra-Base groups had sufficient polymerization at a 4-mm thickness. CONCLUSIONS: Bulk-fill composite demonstrates an even higher degree of polymerization of methacrylate-based flowable composite when applied in a 4-mm thickness.

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