The asymmetric unit of the title compound, C16H13N3O3·0.5C2H6OS, is composed of two independent pyrazolidine-3,5-dione mol-ecules and one dimethyl sulfoxide solvent mol-ecule. In each pyrazolidine-3,5-dione mol-ecule, an intra-molecular N-Hâ¯O hydrogen bond forms an S(5)S(6) motif. In the crystal, pairs of each independent pyrazolidine-3,5-dione mol-ecule are linked by N-Hâ¯O hydrogen bonds, forming dimers with R 2 (2)(8) motifs. These dimers are connected with the other mol-ecules through the solvent mol-ecules via O-Hâ¯O hydrogen bonds, forming ribbons along the b-axis direction. C-Hâ¯Ï inter-actions connect the ribbons. C-Hâ¯O interactions also occur.
(4E)-4-[(2-Hy-droxy-anilino)methyl-idene]-1-phenyl-pyrazolidine-3,5-dione dimethyl sulfoxide hemisolvate.
(4E)-4-[(2-羟基苯胺基)甲基亚甲基]-1-苯基吡唑烷-3,5-二酮二甲基亚砜半溶剂化物
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作者:Akkurt Mehmet, Mohamed Shaaban K, Elremaily Mahmoud A A, Ahmed Eman A, Albayati Mustafa R
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2013 | 起止号: | 2013 Aug 10; 69(Pt 9):o1408-9 |
| doi: | 10.1107/S1600536813022034 | ||
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