In the title compound, C(35)H(24)Cl(2)N(4)O, the phenyl rings are oriented almost parallel to each other, making a dihedral angle of 0.6â (2)°, whereas the chloro-phenyl rings are oriented at a dihedral angle of 28.3â (1)°. The crystal structure is stabilized through an extensive series of C-Hâ¯N, C-Hâ¯O and C-Hâ¯Cl inter-actions. One of the C-Hâ¯N inter-actions generates an R(2) (2)(12) ring motif around a crystallographic inversion centre. C(5), C(10) and C(12) chain motifs are observed in the unit cell through C-Hâ¯N and C-Hâ¯Cl inter-actions. During the structure analysis, it was observed that the unit cell contains large accessible voids, which host disordered solvent mol-ecules. This affects the diffraction pattern, mostly at low scattering angles and was corrected with the SQUEEZE program [Spek, A. L. (2009 â¶). Acta Cryst. D65, 148-155].
2,6-Bis(2-chloro-phen-yl)-4-oxo-3,5-diphenyl-heptane-1,1,7,7-tetra-carbo-nitrile.
2,6-双(2-氯苯基)-4-氧代-3,5-二苯基庚烷-1,1,7,7-四腈
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作者:Ali A Jahubar, Athimoolam S, Bahadur S Asath, Raja V P Alex
| 期刊: | Acta Crystallographica Section E-Structure Reports Online | 影响因子: | 0.600 |
| 时间: | 2011 | 起止号: | 2011 Jun 1; 67(Pt 6):o1407-8 |
| doi: | 10.1107/S1600536811017284 | ||
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