Dissociative Photoionization of Dimethylpyridines and Trimethylpyridine at 266 nm: Dynamics of Methyl Radical Release

266 nm 波长下二甲基吡啶和三甲基吡啶的解离光电离:甲基自由基释放动力学

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Abstract

The 266 nm photolysis of various positional isomers of dimethylpyridines and trimethylpyridine was investigated by measuring the translational energy distribution of the methyl radical following {sp(2)}C-C{sp(3)} bond dissociation. The observed translational energy distribution is attributed to the dissociative photoionization in the cationic ground state following [1 + 1 + 1] three-photon absorption. The translational energy distribution profiles of the methyl radical were broad with the maximum translation energy in excess of 2 eV, which originates due to the dissociation of {sp(2)}C-C{sp(3)} bond ortho to the N atom in the ring. The dynamics of {sp(2)}C-C{sp(3)} bond dissociation in the cationic ground state of methylpyridines is marginally dependent on the number and position of the methyl groups; similar to xylenes, however, it is site-selective with the preferential cleavage of C-C bond in the ortho position to the pyridinic nitrogen atom, which is attributed to the relative stability of the resulting radical cation.

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