Probing the Structural Degradation of CsPbBr(3) Perovskite Nanocrystals in the Presence of H(2)O and H(2)S: How Weak Interactions and HSAB Matter

在H₂O和H₂S存在下探测CsPbBr₃钙钛矿纳米晶体的结构退化:弱相互作用和HSAB的影响

阅读:1

Abstract

Structural degradation of all inorganic CsPbBr(3) in the presence of moisture is considered as one of its major limitations to use as an active component in various light-harvesting and light-emitting devices. Herein, we used two similar molecules, H(2)O and H(2)S, with similar structures, to follow the decomposition mechanism of CsPbBr(3) perovskite nanocrystals. Interestingly, H(2)O acts as a catalyst for the decomposition of CsPbBr(3), which is in contrast to H(2)S. Our experimental observations followed by density functional theory (DFT) calculations showed that the water molecule is intercalated in the CsPbBr(3) perovskite whereas H(2)S is adsorbed in the (100) planes of CsPbBr(3) by a weak electrostatic interaction. According to Pearson's hard-soft acid-base theory, both cations present in CsPbBr(3) prefer soft/intermediate bases. In the case of the water molecule, it lacks a soft base and thus it is not directly involved in the reaction whereas H(2)S can provide a soft base and thus it gets involved in the reaction. Understanding the mechanistic aspects of decomposition can give different methodologies for preventing such unwanted reactions.

特别声明

1、本页面内容包含部分的内容是基于公开信息的合理引用;引用内容仅为补充信息,不代表本站立场。

2、若认为本页面引用内容涉及侵权,请及时与本站联系,我们将第一时间处理。

3、其他媒体/个人如需使用本页面原创内容,需注明“来源:[生知库]”并获得授权;使用引用内容的,需自行联系原作者获得许可。

4、投稿及合作请联系:info@biocloudy.com。